Thermo-Responsive Hydrogel-Coated Gold Nanoshells for In Vivo Drug Delivery

نویسنده

  • Jun-Hyun Kim
چکیده

This paper describes the preparation and characterization of a new type of composite nanoparticle, where the structure consists of a nontoxic hydrogel polymer network that encapsulates a gold shell/silica core. These composite nanoparticles are being developed as photothermally responsive drug-delivery vehicles that undergo structural changes slightly above physiological temperature. A unique property of these nanoparticles is that the hydrogel coatings can be collapsed by exposure to light via excitation of the strong plasmon resonance of the gold shell/silica core; this excitation provides a ready source of heat to the system. Furthermore, the gold nanoshell (GNS) cores were designed to absorb light at near-infrared wavelengths (800–1200 nm), which can pass readily through tissue and water. The thermo-responsive hydrogel coatings were prepared by free radical polymerization of a selected mixture of N-isoproprylacrylamide (NIPAM) and acrylic acid (AAc) in the presence of the GNS core particles. The resultant composite particles were characterized structurally and compositionally by FE-SEM, TEM, and EDX, respectively. UV-vis spectroscopy was used to characterize the optical properties, and DLS was used to determine the average diameter as a function of temperature. As a whole, the results presented here demonstrate that these composite nanoparticles can be reliably prepared and characterized; moreover, their systematic responses to variations in temperature are consistent with their intended use as discrete nanoscale drug-delivery vehicles.

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تاریخ انتشار 2008